Synthesis and structural analysis of beryllium acetylacetonate

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Journal of Beijing University of Chemical Technology ›› 2010, Vol. 37 ›› Issue (4) : 40-43.

材料科学与工程

YANG BingChu;LI WenFang;HUANG XiaoZhong;DU ZuoJuan

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Beryllium acetylacetonate has been synthesized using beryllium oxide, concentrated sulfuric acid and acetylacetone as starting materials. The product was characterized by powder Xray diffraction, elemental analysis, UV visible absorption spectroscopy, Fourier transform infrared spectroscopy, and ¹H nuclear magnetic resonance spectroscopy. The results showed that the strong electron withdrawing effect of Be²⁺ and the ring current of the chelate ring were both clearly observed. The chelate ring formed between Be²⁺and acaccontains conjugate π-bonds which contribute to the stability of Be(acac)₂.

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YANG BingChu;LI WenFang;HUANG XiaoZhong;DU ZuoJuan. Synthesis and structural analysis of beryllium acetylacetonate[J]. Journal of Beijing University of Chemical Technology, 2010, 37(4): 40-43

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2010-03-03	1900-01-01	2010-07-20
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2010-07-20

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