液氦超流转变温度复现性研究

尹亮1 ; 林鹏2; 祁欣1*

北京化工大学学报(自然科学版) ›› 2011, Vol. 38 ›› Issue (1) : 26-29.

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北京化工大学学报(自然科学版) ›› 2011, Vol. 38 ›› Issue (1) : 26-29.
化学与化学工程

液氦超流转变温度复现性研究

  • 尹亮 ; 林鹏; 祁欣*
作者信息 +

Study of the reproducibility of the superfluid transition temperature of helium

  • YIN Liang1; LIN Peng2; QI Xin1*
Author information +
文章历史 +

摘要

利用液氦超流转变时超流氦(He Ⅱ)与正常氦(He Ⅰ)热导率突变的性质复现液氦超流转变温度Tλ。采用带毛细管结构的小型密封瓶,通过控温将微小热流通过小型密封瓶毛细管,实现毛细管中He Ⅰ/He Ⅱ两相共存,并使He Ⅰ/He Ⅱ界面停留在毛细管中,从而获得稳定、平坦的液氦超流转变温坪。利用毛细管热流对液氦超流转变温度的下压效应,得到不同热流的多个温坪,进一步利用外推法求得零热流下真实的Tλ值。24次液氦超流转变温度复现实验结果表明,标准偏差为0.022mK,证明了液氦超流转变温度具有良好的稳定性和复现性,推荐将液氦超流转变温度作为国际温标的固定点使用。

Abstract

Based upon the dramatic change in thermal conductivity of liquid heliumat at the
temperature of the transition between superfluid (He Ⅱ) and normal fluid (He I), a sealed-cell with a capillary has been used to determine the superfluid transition temperature, Tλ. A controlled small heat flow is passed through the capillary of the sealedcell to realize the coexistence of He I and He Ⅱ and maintain the He Ⅰ/He Ⅱ interface in the capillary. A stable and flat lambda transition temperature plateau is obtained. Because there is a depression of Tλ by the heat flow through the capillary, a series of heat flows and several temperature plateaus are made and an extrapolation is applied to determine Tλ with zero heat flow. A rhodiumiron resistance thermometer with series number of A34(RIRT A34)was used in 24 experiments to determine the superfluidtransition temperature with a standard deviation of 0.022mK, which demonstrates the stability and reproducibility of Tλ. We therefore recommend that superfluid transition temperature of helium be used as a fixed point on the International Temperature Scale.

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尹亮1 ; 林鹏2; 祁欣1*
.
液氦超流转变温度复现性研究[J]. 北京化工大学学报(自然科学版), 2011, 38(1): 26-29
YIN Liang1; LIN Peng2; QI Xin1*
.
Study of the reproducibility of the superfluid transition temperature of helium[J]. Journal of Beijing University of Chemical Technology, 2011, 38(1): 26-29

参考文献

[1]张杰, 翁汉元, 吕国会, 等. 中国聚氨酯工业现状及未来发展展望[J]. 新材料产业, 2007 (2): 48-57. 
Zhang J, Wen H Y, Lv G H, et al. A overview of the PU industry present situation and prospects in China[J]. Advanced Materials Industry, 2007(2): 48-
57. (in Chinese)
[2]卫民, 严立楠, 蒋剑春. 木质素及其改性树脂羟值的测定[J]. 生物质化学工程, 2006, 40(5): 18-20. 
Wei M, Yan L N, Jiang J C. Determination of the hydroxyl value of lignin and modified lignin resin[J]. Biomass Chemical Engineering, 2006, 40(5): 18-
20.(in Chinese)
[3]江蓉. 木质素高效率醇化的工艺条件研究[J]. 黄山学院学报, 2008, 10(5): 44-47.Jiang R. Study on the efficient liquefaction of lignin[J]. Journal of Huangshan University, 2008, 10(5): 44-47. (in Chinese)
[4]罗学刚. 高纯木质素提取与热塑改性[M], 北京: 化学工业出版社, 2008. 
Luo X G. High pure lignin extraction and thermoplastic modification[M].Beijing: Chemical Industry Press , 2008. (in Chinese)

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